OneHigh frequency infrared carbon sulfur spectrometerInstrument Overview:
High frequency infrared carbon sulfur analyzerIt can quickly and accurately determine the mass fractions of carbon and sulfur elements in steel, iron, alloys, casting core sand, non-ferrous metals, cement, ore, coke, catalysts, and other materials. This equipment has introduced foreign technology and is a product that integrates optical, mechanical, electrical, computer, and analytical technologies. It has the characteristics of wide measurement range, strong anti-interference ability, complete functions, easy operation, and accurate and reliable analysis results.
IIHigh frequency infrared carbon sulfur spectrometerInfrared detection principle:
CO2、SO2Equipolar molecules have an electric dipole moment, thus possessing structures such as vibration and rotation. Divided into split energy levels according to quantum mechanics, gas molecules can couple with incident characteristic wavelength infrared light to produce absorption. In the infrared light band, gas molecules have selective absorption spectra. When specific wavelengths of infrared light pass throughCO2orSO2After gas, it can produce strong light absorption.
Since the detector converts optical signals into electrical signals, when the detector operates in a linear region, selects a specific wavelength and determines the length of the analysis cell (absorption cell), the concentration of the measured gas in the mixed gas can be calculated by measuring the light intensity. This is the basic principle of infrared absorption method for quantitatively measuring gas concentration. The selected measurement wavelength for this instrument is:CO2by4.26um,SO2by7.4um.
The analysis room includes miniature infrared light sources, mirrors, modulation motors, absorption cells, filters, and detectors. Miniature infrared light source heated by electricity800℃Generate infrared light, which is absorbed by an absorption cellCO2、SO2After absorption, it passes through a narrowband filter to remove the energy of other light radiation outside the above-mentioned wavelength. When it is incident on the detector, what is detected on the detector isCO2、SO2The light intensity corresponding to the concentration is converted into an electrical signal by a detector, and then normalized and calibrated by a microcomputer. The integrated inversion is used to obtain the percentage content of carbon and sulfur elements. A modulation motor is placed between the light source and the absorption cell to modulate the light signal into64HzThe alternating radiation signal. The center frequency of the detector output is64Hz.
The thermoelectric device is converted into an electrical signal, which is then passed through a preamplifier and a preamplifier before entering the microcomputer through digital to analog conversion. In the microcomputer, it undergoes linearization operation to convert it into a signal that isCO2、SO2A numerical value proportional to the content.
IIITechnical specifications and indicators:
1.Basic parameters: Instrument performance and accessories
Determination of Elements | : | Carbon sulfur joint measurement |
Analysis principle | : | High frequency furnace combustion—Infrared absorption method for detection |
Scope of Analysis | : | Carbon:0.0001%-10.0000%(Can be expanded to99.999%) Sulfur:0.0001%-2.0000%(Can be expanded to99.999%) |
Sample size (solid steel standard) | : | standard0.5g |
accuracy of analysis | : | accord withGB/T20123-2006standard accord withISO15350:2000standard |
Sensitivity (maximum reading) | : | C/S:0.1ppm |
Analysis time | : | 20-100Adjustable in seconds (usually35Seconds) |
Work cycle | : | 24hContinuous operation |
High frequency induction heating furnace | : | 1.High frequency furnace output power:2500WFrequency:20MHz 2.Automatic leak detection, outdated and overcurrent alarm 3.electric current/Voltage/power/Selection method for adjusting furnace temperature: suitable for samples of different materials 4.Gas path: High precision flow controller ensures stable airflow and inlet gas path system |
Dust filter | : | 0.4Micro sized ultra microporous metal filter ensures the separation of dust and gas |
Furnace head heating | : | Improve the conversion rate of sulfur and stabilize the sulfur analysis results |
Dust removal system | : | Automatic cleaning: can reduce the impact of dust on analysis results Ash removal system: high-pressure ash removal, * cleaning pipeline dust |
detecting system | : | 1.Circuit design: The whole machine adopts dualCPUModular design of upper and lower computers, selection of lower computersAtmega162To control the microcontroller, the electronic circuit is highly integrated, stable and reliable; 2.Sampling: Using high-speed technology24positionADS1224Sampling chip with high sampling accuracy; 3.Communication: The upper and lower computers adoptUSB2.0Interface communication has improved communication speed; 4.Connection: The infrared detection part is connected to the high-frequency furnaceAgilent1521/2521High speed optical fiberConnection (domestic *), combined with multi-level concealed isolation circuit, * eliminates high-frequency interference; 5.Power supply: Industrial grade integrated linear module power supply, stable output, *; 6.Light source: A specially designed new platinum infrared light source with continuous heating and high spectral efficiency; 7.Analysis pool: gold-plated carbon sulfur analysis pool and high-precision pyroelectric infrared detector; 8.electric machinery: Stepper motor, good thermal stability, continuous service life10Ten thousand hours. |
2.Analysis software
Operating software | : | useDeliphSoftware compilation,WINDOWS XPFull Chinese operating software. |
Analysis Channel | : | Provide channel management function, carbon and sulfur channels can be added, deleted, and edited independently without quantity limit; Pre installed low-carbon and high sulfur interfaces enable automatic software switching. |
Analysis function | : | Analysis processDynamic data integration, per second20Subsampling improves the sensitivity and accuracy of analysis; Provide sample management function, which allows editing of sample names and labels, as well as adding and deleting sample names; The software provides a multi-user management system, which allows administrators to set different user permissions. |
Display function | : | One curve box for carbon and sulfur,Dynamically display real-time data and carbon and sulfur release curves during the analysis process. |
Data processing function | : | The analysis results are based onACCESSDatabase storage, capable of storing all data and curves for each analysis of carbon and sulfur; The analysis results can be freely queried based on various factors such as time, operator, sample name, and identification; Provide curves/Multiple functions including data storage, blank deduction, parameter setting, channel selection, mathematical statistics, result correction, curve comparison, etc; The generation and curve fitting of carbon sulfur working curves can be achieved in software. |
Printing function | : | The printing modes are diversified, providing two printing modes for laboratory and testing stations, and the printing format can be designed by oneself. |
Self diagnostic function | : | The system diagnostic function can be implemented by software to detect the sealing of the furnace head and gas chamber. |
Part Two Supply List
1、 One infrared carbon sulfur analyzer
Serial number | assembly | quantity |
1 | Infrared carbon sulfur analyzer | 1 |
2 | WF-L88High frequency induction combustion furnace | 1 |
3 | Ten thousand electronic balance | 1 |
4 | Tsinghua Tongfang Commercial Microcomputer(18.5LCD) | 1 |
5 | HP1007Laser printer(A4Paper) | 1 |
two.Spare parts list:
name call | gauge grid | single position | number amount | prepare notes |
Pressure relief valve |
| only | 1 | Including specially designed connectors |
tungsten flux | Ultra low carbon sulfur | Kilogram | 1 |
|
Pure iron flux | Ultra low carbon sulfur | bottle | 2 |
|
Quartz tube |
| only | 2 |
|
Dust removal pipe |
| only | 2 |
|
Copper crucible holder |
| only | 1 |
|
Ceramic crucible holder |
| only | 2 |
|
Porcelain crucible | 1000only/box | box | 1 |
|
Stainless steel brush |
| only | 5 |
|
Wire brush |
| only | 1 |
|
Tweezers |
| hold | 1 |
|
Sample key | In the middle | set | 1 | Made of stainless steel |
Flux spoon |
| hold | 1 |
|
tool |
| set | 1 |
|
PVCPipe | 4mm×6mm | rice | 10 |
|
Silicone ring | red | only | 2 |
|
OCircle shape | 13mm×1.9mm | only | 5 |
|
OCircle shape | 37mm×3.1mm | only | 5 |
|
Printing paper |
| book | 1 |
|
Vacuum silicone grease |
| bottle | 1 |
|
Fuse | 4A、20A | only | various4 |
|
Multi purpose socket | 10A | only | 1 |
|
Efficient color changing desiccant | 125g/bottle | bottle | 1 |
|
EfficientCO2absorbent | 125g/bottle | bottle | 1 |
|
Ash discharge pipe | silica gel | root | 1 |
|
Part Three Acceptance terms
1、 Preparation work for acceptance
After the instrument arrives at the site, the user needs to prepare the installation site according to the "User Site Installation Preparation Requirements" provided by the manufacturer, and prepare the power supply (grounding wire), oxygen, power gas, and indoor environment.
After the above conditions are met, notify Party B in writing to arrange for installation engineers to come to the site for installation and debugging.
2、 Instrument unboxing inspection
1.The instrument must be accompanied by a packing list, and the personnel of Party B shall conduct a visual inspection after opening the box to ensure that it is brand new and undamaged.
2.The spare parts and accessories shall be gradually confirmed according to the technical requirements of the supplied goods, and all equipment and materials shall be checked for correctness.
3.The unpacking of instruments and equipment must be accompanied by the engineer of Party A. If any shortage is found, the engineer of Party A shall confirm and be responsible for completing the missing parts within thirty days.
IIIHigh frequency infrared carbon sulfur analyzerAcceptance and assessment methods
1.Repeatability:
Select * Steel Standard Material(The carbon mass fraction is0.400%-1%Within the range, the sulfur mass fraction is0.020%-0.080%Within the scope)One method is to operate according to the operating instructions specified in the instrument manual and conduct continuous testing with a high-frequency furnace7The difference between the maximum and minimum values of the test results should be equal to or greater than1.5r.rCalculate using the following formula:
Carbon:lgr = 0.52121lgω-1.9617
Sulfur:lgr = 0.62212lgω-1.9965
In the formularIndicating repeatability,ωIndicate the calibration value of the substance being tested.
2.Accuracy
Select * (steel or iron) standard substance( The carbon mass fraction is0.003%-4.500%The sulfur mass fraction is0.002%-0.100%Within the range, take three types of samples: high, medium, and low. Operate and calibrate according to the operating method specified in the instrument manual for the high-frequency furnace. After calibration, test each standard substance three times and take the average of the three times. The carbon and sulfur should be equal to or greater thanThe calculated value is shown in the following formula:
In the formula:XRepresenting the average value;
XoIndicate the calibration value of the tested substance;
nIndicate the number of tests conducted;
rExpressing repeatability;
RIndicating reproducibility.
Reproducibility is calculated using the following formula:
Carbon:lgR = 0.58221lgω-1.4558
Sulfur:lgR = 0.68878lgω-1.3693
In the formulaωIndicate the calibration value of the substance being tested.
ISOStandard Error Comparison Table
Carbon:ISO9556 | sulfur: ISO4935 | ||||
%(M/M) | Repeatabilityr | ReproducibilityR | %(M/M) | Repeatabilityr | ReproducibilityR |
0.003 | 0.00053 | 0.00119 | 0.002 | 0.00021 | 0.00059 |
0.005 | 0.00069 | 0.00160 | 0.005 | 0.00037 | 0.00111 |
0.01 | 0.00099 | 0.00240 | 0.008 | 0.0005 | 0.00153 |
0.015 | 0.00122 | 0.00304 | 0.010 | 0.00057 | 0.00179 |
0.02 | 0.00142 | 0.00359 | 0.015 | 0.00074 | 0.00236 |
0.03 | 0.00176 | 0.00455 | 0.020 | 0.00088 | 0.00289 |
0.04 | 0.00204 | 0.00537 | 0.030 | 0.00114 | 0.00382 |
0.05 | 0.00229 | 0.00612 | 0.040 | 0.00136 | 0.00465 |
0.06 | 0.00252 | 0.00680 | 0.050 | 0.00156 | 0.00543 |
0.08 | 0.00293 | 0.00805 | 0.060 | 0.00175 | 0.00615 |
0.10 | 0.00329 | 0.00916 | 0.070 | 0.00193 | 0.00684 |
0.15 | 0.00406 | 0.01160 | 0.080 | 0.00209 | 0.00750 |
0.20 | 0.00472 | 0.01372 | 0.090 | 0.00225 | 0.00814 |
0.30 | 0.00583 | 0.01737 | 0.100 | 0.00241 | 0.00875 |
0.50 | 0.00761 | 0.02338 | 0.150 | 0.00310 | 0.01157 |
1.0 | 0.01092 | 0.03501 | 0.200 | 0.00370 | 0.01410 |
1.5 | 0.01349 | 0.04433 | 0.300 | 0.00477 | 0.01864 |
2.0 | 0.01567 | 0.05242 |
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3.0 | 0.01936 | 0.06637 |
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4.5 | 0.02392 | 0.08404 |
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6.0 | 0.02779 | 0.09937 |
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Part Four train
1、 On site technical training
The first party is responsible for providing training to the personnel of the second party on operation, maintenance, daily malfunctions, etc., to ensure that the personnel of the second party can use the instruments immediately and quickly put them into production use.
2、 System training
The second party may also send personnel to the first party for system training. Training personnel2People, for a period of time5The specific training time will be determined through negotiation between both parties, and transportation, accommodation, and meals will be provided by oneself. The training content includes:
- Analysis principle and method of carbon sulfur analyzer;
- The structure and characteristics of the Jiebo series carbon and sulfur instruments;
- Quantitative analysis of carbon and sulfur analyzer (with a focus on steel materials);
- Setting analysis conditions, working curves, calibration, etc;
- Troubleshooting of daily malfunctions;
- Maintenance and upkeep of instruments.
Part Five Technology and after-sales service
1. After sales service is provided byBeijing Zhongye Yiyuan Technology Co., LtdDirectly responsible.
2. From the date of shipment of the instrument,Free one-year warranty for the entire machineLifetime service and long-term provision of various spare parts.
3. When users encounter problems, after-sales service personnel will24Provide guidance and resolution through fax within the time frame.
4. When it is confirmed that the instrument has malfunctioned and requires on-site maintenance,1000Within kilometers, the area should not exceed2Arrived within one working day,1000Areas beyond kilometers shall not exceed3Arrive within one working day; In case of special circumstances, it is necessary to arrive within the agreed time with the customer.
5. The content of on-site maintenance services: repairing instrument malfunctions; Testing instrument indicators; Training function operation; Introduce usage experience and troubleshooting.
6. Regularly providing service communication to users: introducing development trends and new technological features of instruments; Introduce testing reports and user experience from various industries.